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Full text of "Practical Organic Chemistry"

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CONTENTS

PREPARATIONS—                                                                    PAGE
Dehydration of liquids..............     56
Determination of specific gravity     .........     56
„              boiling-point..........     58
Ether......................     59
Purification of commercial ether     .........     61
Ethylene bromide.................     62
Acetaldehyde...................     64
Methyl alcohol..................     67
•Methyl iodide...................     68
Amyl alcohol...................     69
• Amyl nitrite....................     69
Acetone....................,   .     69
Chloroform....................     70
Acetoxime....................     71
Melting-point determination............     72
Acetic acid....................     74
Acetyl chloride..................     74
Acetic anhydride................'..     76
• Acetamide....................     77
Heating under pressure............ . . .     78
Acetonitrile....................     79
Methylamine hydrochloride (Hermann's reaction) ...     80
v Ethyl acetate . ..................     Si
Ethyl acetoacetate .................     83
Distillation in vacuo...............     84
Monochloracetic acid...............     87
Monobromacetic acid...............     89
Glycocoll.....................     90
Glycocoll ester hydrochloride........• ....     92
Preparation of hydrogen chloride.........     93
Diazoacetic ester.................     94
Diethyl malonate.................     96
Ethyl malonic acid.................     97
Chloral hydrate..................     99
Trichloracetic acid .......«........     99
•  Oxalic acid   .  „..................    loo